Determination of the heat of combustion of benzoic acid using stand material

VC4.3.3.1_s
Determination of the heat of combustion of benzoic acid using stand material
Determination of the heat of combustion of benzoic acid using stand material

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Description

In experiment C4.3.3.1, the temperature rise in the demonstration calorimeter is measured while burning benzoic acid. The substance is weighed before and after the combustion process. The combustion takes place in an oxygen atmosphere, whereby ignition is initiated by a filament. The energy released is calculated using either a previously determined heat capacity of the filled calorimeter or the individual theoretical values of the heat capacities of the glass jacket and calorimeter liquid. The quantity of heat Q is calculated according to the following formula:

Here DT is the measured temperature difference, mk and m(H2O) are the mass of the calorimeter and of the water and Ck and C(H2O) is the heat capacity of the glass apparatus and the water. In order to calculate the heat of combustion DH, the ignition energy, which also contributed to the heating of the apparatus, must be subtracted and the quantity of heat must be expressed relative to one mol of substance.

Variant (a) is set up in a chemistry board system frame and variant (b) is set up on a base rail.

Components of equipment sets

1 667325 Calorimeter for solids and liquids LD
4 664800  8  Gas scrubber bottle, lower section, 200 ml LD
4 664805  8  Glass tube insert, ST 29/32 LD
4 665392  4  Joint clip plastic, ST 29/32 LD
1 666603  4  Base rail, 95 cm LD
8 30109  4  Bosshead S LD
4 666615  4  Universal bosshead LD
2 30172  4  Universal clamp, 0...120 mm LD
5 666555  4  Universal clamp 0...80 mm LD
4 30127  4  Stand rod 50 cm, 10 mm Ø LD
1 524013  8  Sensor-CASSY 2 LD
1 524220  4  CASSY Lab 2 LD
1 5240673  4  NiCr-Ni adapter S, type K LD
1 529676  4  Temperature probe, NiCr-Ni, 1.5 mm, type K LD
1 667183  4  Rubber tubing Ø 8 mm, t = 2 mm, l = 1m LD
1 667197  4  Silicone tubing, 4 mm diam., 1 m LD
1 604510  4  Tubing connector, 4...15 mm LD
1 521536  4  DC Power Supply 2 x 0...16 V/2 x 0...5 A LD
1 521231  8  Low-voltage power supply 3/6/9/12 V LD
1 6668191 Stirring top, with GL 32 screw th LD
3 500421  4  Connecting lead 19 A, 50 cm, red LD
3 500422  4  Connecting lead 19 A, 50 cm, blue LD
1 660998  4  Minican pressurised gas canister, oxygen LD
GHS03GHS04 Danger H270 H280
1 660980  4  Fine regulating valve for minican gas canisters LD
1 608360  4  Pestle, 54 mm long LD
1 667092  4  Mortar 30 ml, 56 mm x 36 mm LD
1 ADAHCB3001  4  Precision Balance, 3000 g / 0,1 g LD
1 ADAHCB602H Precision Balance, 600 g /0,01g, with USB interface LD
1 6708300  4  Benzoic acid, 50 g LD
GHS07 Warning H302 H319
1 6738420  4  Sodium hydroxide solution, 1 mol/l, 500 ml LD
GHS05 Danger H314 H290
1 6747850  4  Sulfuric acid, 95-98 %, 250 ml LD
GHS05 Danger H314 H290
1 additionally required:
PC with Windows XP/Vista/7/8/10 (x86 or x64)

Experiment Instructions

PDF (Experiment description) PDF (Experiment description) C4.3.3.1 Determination of the heat of combustion of benzoic acid
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